NickelMaghrebV1, Main, Exploration, bibRecord, 000957

Reactive magnetron sputtering as a way to improve the knowledge of metastable f.c.c. nitrogen solid solutions formed during plasma assisted nitriding of Inconel 690

Identifieur interne : 000957 ( Main/Exploration ); précédent : 000956; suivant : 000958

Reactive magnetron sputtering as a way to improve the knowledge of metastable f.c.c. nitrogen solid solutions formed during plasma assisted nitriding of Inconel 690

Auteurs : T. Czerwiec [France] ; H. He [France, République populaire de Chine] ; A. Saker [Algérie] ; L. Tran Huu [France] ; C. Dong [République populaire de Chine] ; C. Frantz [France] ; H. Michel [France]

Source :

Surface & coatings technology [ 0257-8972 ] ; 2003.

RBID : Pascal:04-0503490

Descripteurs français

Pascal (Inist)
- Traitement surface, Plasma.

English descriptors

KwdEn :
- Plasma, Surface treatment.

Abstract

Low temperature plasma assisted nitriding (PAN) treatments of Inconel 690 (a nickel base alloy with a 30 wt.% chromium content) produce a complex layer constituted by two different metastable f.c.c. solid solutions denoted (γ_N1 and γ_N2). In addition, different layer thicknesses are observed for differently oriented grains. Reactive magnetron sputtering (RMS) of Inconel 690 in argon-nitrogen containing mixtures is used to produce homogeneous films constituted by a well defined γ_N phase. In reactive conditions, the as-deposited coatings (T< 100 °C) containing up to 30 at.% of nitrogen are nanocrystalline supersaturated f.c.c. solid solution (γ_N) with a grain size lying between 3 and 7.5 nm. A comparison between the products synthesized by these two techniques (PAN and RMS) is presented in this study. The formation of γ_N phases in low temperature PAN is discussed in the light of electron backscatter diffraction measurements and by comparison with X-ray diffraction patterns of RMS coatings. By using the results obtained in situ by RMS on heated substrates and by tempering of as-deposited films, the decomposition products of the γ_N phase at high temperature (>450 °C) or long PAN treatments at 400 °C are identified to be f.c.c. CrN and γ(Ni,Fe) depleted in nitrogen.

Affiliations:

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Le document en format XML

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<series><title level="j" type="main">Surface & coatings technology</title>
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<front><div type="abstract" xml:lang="en">Low temperature plasma assisted nitriding (PAN) treatments of Inconel 690 (a nickel base alloy with a 30 wt.% chromium content) produce a complex layer constituted by two different metastable f.c.c. solid solutions denoted (γ<sub>N1</sub>
 and γ<sub>N2</sub>
). In addition, different layer thicknesses are observed for differently oriented grains. Reactive magnetron sputtering (RMS) of Inconel 690 in argon-nitrogen containing mixtures is used to produce homogeneous films constituted by a well defined γ<sub>N</sub>
 phase. In reactive conditions, the as-deposited coatings (T< 100 °C) containing up to 30 at.% of nitrogen are nanocrystalline supersaturated f.c.c. solid solution (γ<sub>N</sub>
) with a grain size lying between 3 and 7.5 nm. A comparison between the products synthesized by these two techniques (PAN and RMS) is presented in this study. The formation of γ<sub>N</sub>
 phases in low temperature PAN is discussed in the light of electron backscatter diffraction measurements and by comparison with X-ray diffraction patterns of RMS coatings. By using the results obtained in situ by RMS on heated substrates and by tempering of as-deposited films, the decomposition products of the γ<sub>N</sub>
 phase at high temperature (>450 °C) or long PAN treatments at 400 °C are identified to be f.c.c. CrN and γ(Ni,Fe) depleted in nitrogen.</div>
</front>
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Reactive magnetron sputtering as a way to improve the knowledge of metastable f.c.c. nitrogen solid solutions formed during plasma assisted nitriding of Inconel 690

Reactive magnetron sputtering as a way to improve the knowledge of metastable f.c.c. nitrogen solid solutions formed during plasma assisted nitriding of Inconel 690

Source :

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Le document en format XML

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Pour mettre un lien sur cette page dans le réseau Wicri